Issue 27, 2010
From the journal:

Chemical Communications

A novel synthesis of calix[4]thiophenes and calix[4]furans†

Gon-Ann Lee,*a   Wen-Chieh Wang,a   Minghuey Shiehb  and  Ting-Shen Kuob  

* Corresponding authors

a Department of Chemistry, Fu Jen Catholic University, Hsinchuang, Taiwan, Republic of China
E-mail: 016850@mail.fju.edu.tw

b Department of Chemistry, National Taiwan Normal University, Taiwan

Abstract

The addition of heteroaryllithium to various ketones followed by dehydration gave 1-(2-heteroaryl)cycloalkenes and (2-hetero- aryl)alkenes. When alkenes were treated with 10 mol% NIS, calix[4]thiophenes and calix[4]furans were obtained in good yields.

Graphical abstract: A novel synthesis of calix[4]thiophenes and calix[4]furans

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Article information

DOI
https://doi.org/10.1039/C0CC00437E
Article type
Communication
Submitted
17 Mar 2010
Accepted
12 May 2010
First published
03 Jun 2010

Chem. Commun., 2010,46, 5009-5011

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A novel synthesis of calix[4]thiophenes and calix[4]furans

G. Lee, W. Wang, M. Shieh and T. Kuo, Chem. Commun., 2010, 46, 5009 DOI: 10.1039/C0CC00437E

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