SCHEDULED MAINTENANCE
Spontaneous symmetry breaking during interrupted crystallization of an axially chiral amino acid derivative†
Abstract
High net enantiomeric excess was observed for crystal collections obtained by
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Supplementary files
- All synthetic procedures (including three step preparation of 1 from m-anisic acid) and chracterization data for prepared compounds, details for crystallization of 3-TFA, X-ray diffraction data (CIF) for 1 and 3-TFA, NMR spectra for all compounds, HPLC analysis methods. PDF (16563K)
- Crystal structure data TXT (39K)
Article information
- Article type
- Communication
- Submitted
- 21 Oct 2009
- Accepted
- 04 Feb 2010
- First published
- 19 Feb 2010
Chem. Commun., 2010,46, 2094-2096
Permissions
Spontaneous symmetry breaking during interrupted crystallization of an axially chiral amino acid derivative
M. A. Sephton, C. R. Emerson, L. N. Zakharov and P. R. Blakemore, Chem. Commun., 2010, 46, 2094 DOI: 10.1039/B922028C
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