Issue 23, 2009
From the journal:

Organic & Biomolecular Chemistry

Synthesis of a photo-caged aminooxy alkane thiol†

Rock J. Mancini,a   Ronald C. Li,a   Zachary P. Tolstykaa  and  Heather D. Maynard*a  

* Corresponding authors

a Department of Chemistry and Biochemistry, University of California, Los Angeles, 607 Charles E. Young Drive South, Los Angeles, U. S. A
E-mail: maynard@chem.ucla.edu
Fax: +1-310-206-3403
Tel: +1-310- 267-5162

Abstract

A photo-caged aminooxy alkane thiol synthesized in 7 steps and 15% overall yield was used to form a self-assembled monolayer (SAM). Photo-deprotection on the surface was confirmed by FT-IR spectroscopy and contact angle goniometry. Conjugation of a small molecule ketone, ethyl levulinate, further confirmed the presence of aminooxy groups on the surface.

Graphical abstract: Synthesis of a photo-caged aminooxy alkane thiol

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Article information

DOI
https://doi.org/10.1039/B904195H
Article type
Paper
Submitted
02 Mar 2009
Accepted
08 Sep 2009
First published
06 Oct 2009

Org. Biomol. Chem., 2009,7, 4954-4959

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Synthesis of a photo-caged aminooxy alkane thiol

R. J. Mancini, R. C. Li, Z. P. Tolstyka and H. D. Maynard, Org. Biomol. Chem., 2009, 7, 4954 DOI: 10.1039/B904195H

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