Issue 12, 2009
From the journal:

Dalton Transactions

Synthesis of the nickel selenophosphinates [Ni(Se2PR2)2] (R = iPr, tBu and Ph) and their use as single source precursors for the deposition of nickel phosphide or nickel selenide nanoparticles†

Weerakanya Maneeprakorn,a   Chinh Q. Nguyen,a   Mohammad A. Malik,a   Paul O'Brien*a  and  James Rafterya  

* Corresponding authors

a The School of Chemistry and the School of Materials, The University of Manchester, Oxford Road, Manchester, UK
E-mail: paul.obrien@manchester.ac.uk
Fax: 44 161 275 4598
Tel: 44 161 275 4653

Abstract

Nickel phosphide (Ni2P and Ni12P5) or nickel selenide (NiSe) nanoparticles were prepared from the single molecule precursor, dialkyldiselenophosphinato nickel(II), [Ni(Se2PR2)2] (R = iPr, tBu and Ph) by thermolysis in trioctylphosphine oxide (TOPO) or hexadecylamine (HDA). The chemical composition of these nanoparticles depends on the precursors, capping agents, and reaction temperature.

Graphical abstract: Synthesis of the nickel selenophosphinates [Ni(Se2PR2)2] (R = iPr, tBu and Ph) and their use as single source precursors for the deposition of nickel phosphide or nickel selenide nanoparticles

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Article information

DOI
https://doi.org/10.1039/B816903A
Article type
Paper
Submitted
29 Sep 2008
Accepted
09 Jan 2009
First published
05 Feb 2009

Dalton Trans., 2009, 2103-2108

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Synthesis of the nickel selenophosphinates [Ni(Se2PR2)2] (R = iPr, tBu and Ph) and their use as single source precursors for the deposition of nickel phosphide or nickel selenide nanoparticles

W. Maneeprakorn, C. Q. Nguyen, M. A. Malik, P. O'Brien and J. Raftery, Dalton Trans., 2009, 2103 DOI: 10.1039/B816903A

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