Issue 39, 2008
From the journal:

Chemical Communications

Selected regiocontrolled transformations applied to the synthesis of (1S)-cis-chrysanthemic acid from (1S)-3,4-epoxy-2,2,5,5-tetramethylcyclohexanol†

Alain Krief,*a   Humaira Y. Gondalab  and  Adrian Kremera  

* Corresponding authors

a Laboratoire de Chimie Organique de Synthèse, Facultés Universitaires N.-D. de la Paix, 61 rue de Bruxelles, Namur, Belgium
E-mail: alain.krief@fundp.ac.be
Fax: +32 (81)724536
Tel: +32 (81)724539

b On leave from the Chemistry department of the University of Sargodha, Pakistan

Abstract

(1S)-cis-Chrysanthemic acid has been prepared in a few steps with complete control of the relative and absolute stereochemistry using regiocontrolled epoxide ring opening, diol mono-oxidation and cyclopropanation.

Graphical abstract: Selected regiocontrolled transformations applied to the synthesis of (1S)-cis-chrysanthemic acid from (1S)-3,4-epoxy-2,2,5,5-tetramethylcyclohexanol

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Article information

DOI
https://doi.org/10.1039/B808695H
Article type
Communication
Submitted
22 May 2008
Accepted
10 Jul 2008
First published
26 Aug 2008

Chem. Commun., 2008, 4753-4755

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Selected regiocontrolled transformations applied to the synthesis of (1S)-cis-chrysanthemic acid from (1S)-3,4-epoxy-2,2,5,5-tetramethylcyclohexanol

A. Krief, H. Y. Gondal and A. Kremer, Chem. Commun., 2008, 4753 DOI: 10.1039/B808695H

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