Issue 26, 2008
From the journal:

Chemical Communications

Safe, facile radical-based reduction and hydrosilylation reactions in a microreactor using tris(trimethylsilyl)silane

Arjan Odedra,a   Karolin Geyer,a   Tomas Gustafsson,a   Ryan Gilmoura  and  Peter H. Seeberger*a  

* Corresponding authors

a Laboratory for Organic Chemistry, Swiss Federal Institute of Technology (ETH) Zurich, Wolfgang-Pauli-Strasse 10, Zurich, Switzerland
E-mail: seeberger@org.chem.ethz.ch
Fax: +41 44 633 1235
Tel: +41 44 633 2103

Abstract

A highly efficient system for tris(trimethylsilyl)silane (TTMSS) mediated deoxygenation, dehalogenation and hydrosilylation reactions is described in a microstructured device; this convenient platform enables the scale up of radical-based processes.

Graphical abstract: Safe, facile radical-based reduction and hydrosilylation reactions in a microreactor using tris(trimethylsilyl)silane

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Article information

DOI
https://doi.org/10.1039/B803715A
Article type
Communication
Submitted
04 Mar 2008
Accepted
27 Mar 2008
First published
29 Apr 2008

Chem. Commun., 2008, 3025-3027

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Safe, facile radical-based reduction and hydrosilylation reactions in a microreactor using tris(trimethylsilyl)silane

A. Odedra, K. Geyer, T. Gustafsson, R. Gilmour and P. H. Seeberger, Chem. Commun., 2008, 3025 DOI: 10.1039/B803715A

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