Real-time monitoring of a dynamic molecular system using 1H-13C HSQC NMR spectroscopy with an optimized 13C window

Giulio Gasparini; Bruno Vitorge; Paolo Scrimin; Damien Jeannerat; Leonard J. Prins

doi:10.1039/B803074J

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Real-time monitoring of a dynamic molecular system using ¹H-¹³C HSQCNMR spectroscopy with an optimized ¹³C window†

Giulio Gasparini,‡^a Bruno Vitorge,‡^b Paolo Scrimin,^a Damien Jeannerat*^b and Leonard J. Prins*^a

Author affiliations

* Corresponding authors

^a Department of Chemical Sciences and CNR ITM Padova Section, University of Padova, via Marzolo 1, Padova, Italy
E-mail: leonard.prins@unipd.it
Fax: +39 049 8275239
Tel: +39 049 8275256

^b Department of Organic Chemistry, University of Geneva, 30 Quai E Anserment, Geneva, Switzerland
E-mail: Damien.Jeannerat@chiorg.unige.ch

Abstract

The kinetic and thermodynamic parameters of an equilibrating network involving 8 molecules can be determined from a series of quick and highly resolved ¹H-¹³C HSQC NMR experiments obtained using a reduced carbon spectral window.

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Supplementary files

Characterization data for hydrazones 1C and 1D, procedure for measuring the ¹H- ¹³C HSQC NMR spectra, quantification of signals in the HSQC spectra and Scientist model files for fitting the kinetics PDF (88K)

Article information

DOI: https://doi.org/10.1039/B803074J
Article type: Communication
Submitted: 21 Feb 2008
Accepted: 17 Mar 2008
First published: 21 Apr 2008

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Chem. Commun., 2008, 3034-3036

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Real-time monitoring of a dynamic molecular system using ¹H-¹³C HSQC NMR spectroscopy with an optimized ¹³C window

G. Gasparini, B. Vitorge, P. Scrimin, D. Jeannerat and L. J. Prins, Chem. Commun., 2008, 3034 DOI: 10.1039/B803074J

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