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Issue 9, 2007
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Solvent inclusion in the structural voids of form II carbamazepine: single-crystal X-ray diffraction, NMR spectroscopy and Hirshfeld surface analysis

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Abstract

Single-crystal X-ray diffraction and solution 1H NMR spectroscopy, in conjunction with Hirshfeld surface analysis, give evidence of solvent inclusion in the trigonal polymorph of carbamazepine, which in the unsolvated form is characterised by the presence of large structural voids.

Graphical abstract: Solvent inclusion in the structural voids of form II carbamazepine: single-crystal X-ray diffraction, NMR spectroscopy and Hirshfeld surface analysis

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Supplementary files

Article information


Submitted
31 May 2007
Accepted
06 Jun 2007
First published
25 Jun 2007

CrystEngComm, 2007,9, 728-731
Article type
Communication

Solvent inclusion in the structural voids of form II carbamazepine: single-crystal X-ray diffraction, NMR spectroscopy and Hirshfeld surface analysis

F. P. A. Fabbiani, L. T. Byrne, J. J. McKinnon and M. A. Spackman, CrystEngComm, 2007, 9, 728
DOI: 10.1039/B708303N

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