Issue 47, 2007
From the journal:

Chemical Communications

A diastereoselective carbocyclisation of allene-hydrazones through the intramolecular allylic transfer reaction†

Sang-Hoon Kim,a   Seung-Ju Oh,a   Yurim Kima  and  Chan-Mo Yu*a  

* Corresponding authors

a BK-21 School of Chemical Materials Science and Department of Chemistry, Sungkyunkwan University, Korea
E-mail: cmyu@chem.skku.ac.kr
Fax: +82 31 290 7075
Tel: +82 31 290 7067

Abstract

A diastereoselective synthesis of cyclic hydrazines was achieved from a carbocyclisation of allene-hydrazones by the Pd-catalyzed distannylation of an allene moiety, followed by the transmetallation of allylic stannane intermediates with TiCl4.

Graphical abstract: A diastereoselective carbocyclisation of allene-hydrazones through the intramolecular allylic transfer reaction

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Article information

DOI
https://doi.org/10.1039/B712856H
Article type
Communication
Submitted
21 Aug 2007
Accepted
18 Sep 2007
First published
03 Oct 2007

Chem. Commun., 2007, 5025-5027

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A diastereoselective carbocyclisation of allene-hydrazones through the intramolecular allylic transfer reaction

S. Kim, S. Oh, Y. Kim and C. Yu, Chem. Commun., 2007, 5025 DOI: 10.1039/B712856H

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