Issue 13, 2006
From the journal:

Organic & Biomolecular Chemistry

Highly efficient hydrazination of conjugated nitroalkenesviaimidazole or DMAP mediated Morita–Baylis–Hillman reaction†‡

Mamta Dadwal,a   Shaikh M. Mobinb  and  Irishi N. N. Namboothiri*a  

* Corresponding authors

a Department of Chemistry, Indian Institute of Technology, Bombay, Mumbai, India
E-mail: irishi@iitb.ac.in
Fax: +91 22 2576 7152
Tel: +91 22 2576 7196

b National Single Crystal X-ray Diffraction Facility, Indian Institute of Technology, Bombay, Mumbai, India

Abstract

Novel α-hydrazino-α,β-unsaturated nitroalkenes, which exhibit dynamic phenomenon on the NMR time scale, were synthesized in excellent yields via imidazole or DMAP mediated Morita–Baylis–Hillman (MBH) type reaction of nitroalkenes with azodicarboxylates.

Graphical abstract: Highly efficient hydrazination of conjugated nitroalkenes via imidazole or DMAP mediated Morita–Baylis–Hillman reaction

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Article information

DOI
https://doi.org/10.1039/B604899D
Article type
Communication
Submitted
04 Apr 2006
Accepted
22 May 2006
First published
31 May 2006

Org. Biomol. Chem., 2006,4, 2525-2528

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Highly efficient hydrazination of conjugated nitroalkenes via imidazole or DMAP mediated Morita–Baylis–Hillman reaction

M. Dadwal, S. M. Mobin and I. N. N. Namboothiri, Org. Biomol. Chem., 2006, 4, 2525 DOI: 10.1039/B604899D

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