Issue 18, 2006
From the journal:

Chemical Communications

Through-bond homonuclear correlation experiments in solid-state NMR applied to quadrupolar nuclei in Al–O–P–O–Al chains†

Michaël Deschamps,*a   Franck Fayon,a   Valérie Montouillouta  and  Dominique Massiota  

* Corresponding authors

a CRMHT-CNRS, 1D, Avenue de la Recherche Scientifique, Orléans cedex 2, France
E-mail: deschamps@cnrs-orleans.fr
Fax: +33 (0)2 38 63 81 03
Tel: +33 (0)2 38 25 55 11

Abstract

Through-bond homonuclear correlation experiments can be realised in solids between spins of type X, separated by four chemical bonds, in X–O–Y–O–X motifs, provided a J coupling between X and Y exists: central transitions of quadrupolar 27Al spins can be correlated via the J2 scalar coupling between 27Al (X) and 31P (Y) in materials featuring Al–O–P–O–Al motifs.

Graphical abstract: Through-bond homonuclear correlation experiments in solid-state NMR applied to quadrupolar nuclei in Al–O–P–O–Al chains

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Article information

DOI
https://doi.org/10.1039/B600514D
Article type
Communication
Submitted
13 Jan 2006
Accepted
09 Mar 2006
First published
21 Mar 2006

Chem. Commun., 2006, 1924-1925

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Through-bond homonuclear correlation experiments in solid-state NMR applied to quadrupolar nuclei in Al–O–P–O–Al chains

M. Deschamps, F. Fayon, V. Montouillout and D. Massiot, Chem. Commun., 2006, 1924 DOI: 10.1039/B600514D

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