Issue 4, 2005
From the journal:

Green Chemistry

A new method for the synthesis of triaryl phosphates

Gheorghe Ilia,*a   Smaranda Iliescua  and  Adriana Popaa  

* Corresponding authors

a Romanian Academy, Institute of Chemistry Timisoara, 24 Mihai Viteazul Bd, Timisoara, Romania
E-mail: ilia@acad-icht.tm.edu.ro
Fax: +40256491824

Abstract

Triaryl phosphates were obtained by a new, efficient and environmentally friendly method, the vapor–liquid condensation of phosphorus oxychloride with hydroxyaryl compounds. Phosphorus oxychloride was heated and carried by a stream of nitrogen into a solution containing 20% aqueous sodium hydroxide and hydroxyaryl compound. Triaryl phosphates obtained as the solid products were separated by filtration, purified, dried under vacuum and characterized by IR, 1H-NMR, 31P-NMR and HPLC.

Graphical abstract: A new method for the synthesis of triaryl phosphates

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Article information

DOI
https://doi.org/10.1039/B417264G
Article type
Paper
Submitted
12 Nov 2004
Accepted
17 Feb 2005
First published
25 Feb 2005

Green Chem., 2005,7, 217-218

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A new method for the synthesis of triaryl phosphates

G. Ilia, S. Iliescu and A. Popa, Green Chem., 2005, 7, 217 DOI: 10.1039/B417264G

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