Issue 27, 2005

A very sensitive high-resolution NMR method for quadrupolar nuclei: SPAM-DQF-STMAS

Abstract

We show that by combining the intrinsically larger (with respect to MQMAS) efficiency of Double-Quantum Filtered Satellite-Transition MAS (DQF-STMAS), with the large S/N gain of the Soft-Pulse Added Mixing (SPAM) concept, a new very sensitive high-resolution solid-state NMR method can be obtained for semi-integer quadrupolar nuclei.

Graphical abstract: A very sensitive high-resolution NMR method for quadrupolar nuclei: SPAM-DQF-STMAS

Article information

Article type
Communication
Submitted
24 Feb 2005
Accepted
17 May 2005
First published
09 Jun 2005

Chem. Commun., 2005, 3472-3474

A very sensitive high-resolution NMR method for quadrupolar nuclei: SPAM-DQF-STMAS

J. Amoureux, A. Flambard, L. Delevoye and L. Montagne, Chem. Commun., 2005, 3472 DOI: 10.1039/B502840J

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