Issue 6, 2004
From the journal:

Mendeleev Communications

Kinetic resolution of 1-methyl- and 1-phenyl-3-amino-1,2-dicarba-closo-dodecaboranes via acylation with chiral acyl chlorides

Galina L. Levit,*a   Victor P. Krasnov,a   Alexander M. Demin,a   Mikhail I. Kodess,a   Liliya Sh. Sadretdinova,a   Tatyana V. Matveeva,a   Valentina A. Ol'shevskaya,b   Valery N. Kalinin,b   Oleg N. Chupakhina  and  Valery N. Charushina  

* Corresponding authors

a I.Ya. Postovsky Institute of Organic Synthesis, Ural Branch of the Russian Academy of Sciences, Ekaterinburg, Russian Federation, , Ekaterinburg, Russian Federation
E-mail: ca512@ios.uran.ru

b A.N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow, Russian Federation, ul. Vavilova, 28, Moscow, Russian Federation

Abstract

A study of the kinetic resolution of racemic 1-substituted 3-amino-1,2-dicarba-closo-dodecaboranes by chiral acyl chlorides has shown that N-tosyl-(S)-prolyl and N-phthaloyl-(S)-alaninyl chlorides are more efficient resolving agents than (S)-naproxen chloride.

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Article information

DOI
https://doi.org/10.1070/MC2004v014n06ABEH002047
Article type
Communication
Submitted
27 Sep 2004

Mendeleev Commun., 2004,14, 293-295

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Kinetic resolution of 1-methyl- and 1-phenyl-3-amino-1,2-dicarba-closo-dodecaboranes via acylation with chiral acyl chlorides

G. L. Levit, V. P. Krasnov, A. M. Demin, M. I. Kodess, L. Sh. Sadretdinova, T. V. Matveeva, V. A. Ol'shevskaya, V. N. Kalinin, O. N. Chupakhin and V. N. Charushin, Mendeleev Commun., 2004, 14, 293 DOI: 10.1070/MC2004v014n06ABEH002047

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