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Issue 10, 2003
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A novel and direct synthesis of alkylated 2,2′-bithiophene derivatives using a combination of hypervalent iodine(III) reagent and BF3·Et2O

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Abstract

A novel nonmetallic oxidative coupling of alkylthiophene derivatives leading to the corresponding 2,2′-bithiophene derivatives using a combination of a hypervalent iodine(III) reagent, phenyliodine bis(trifluoroacetate) (PIFA), and BF3·Et2O was developed.

Graphical abstract: A novel and direct synthesis of alkylated 2,2′-bithiophene derivatives using a combination of hypervalent iodine(iii) reagent and BF3·Et2O

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Publication details

The article was received on 05 Mar 2003, accepted on 24 Apr 2003 and first published on 29 Apr 2003


Article type: Communication
DOI: 10.1039/B302462H
Org. Biomol. Chem., 2003,1, 1647-1649

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    A novel and direct synthesis of alkylated 2,2′-bithiophene derivatives using a combination of hypervalent iodine(III) reagent and BF3·Et2O

    H. Tohma, M. Iwata, T. Maegawa, Y. Kiyono, A. Maruyama and Y. Kita, Org. Biomol. Chem., 2003, 1, 1647
    DOI: 10.1039/B302462H

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