2,6-Dimethylphenols and 5,5'-dimethyl-6,6'-spirobiindanol react with diethylphosphite to give phosphates, which are easily transformed by LDA to (o-hydroxyphenyl)methylphosphonates.
New synthetic approach to (o-hydroxyphenyl)methylphosphonic acid derivatives
G. A. Consiglio, S. Failla and P. Finocchiaro, Mendeleev Commun., 2003, 13, 182 DOI: 10.1070/MC2003v013n04ABEH001784
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