1,2,4-Triazinylcarboranes: a new approach to the synthesis and the crystal structures of 1-(3,6-ditolyl-1,2,4-triazin-5-yl)-2-phenyl-1,2-dicarba-closo-dodecaborane and 1,7-bis[6-phenyl-3-(4-chlorophenyl)-1,2,4-triazin-5-yl]-1,7-dicarba-closo-dodecaborane

Oleg N. Chupakhin; Anton M. Prokhorov; Dmitry N. Kozhevnikov; Vladimir L. Rusinov; Valery N. Kalinin; Valentina A. Olshevskaya; Ivan V. Glukhov; Mikhail Yu. Antipin

doi:10.1070/MC2003v013n04ABEH001773

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1,2,4-Triazinylcarboranes: a new approach to the synthesis and the crystal structures of 1-(3,6-ditolyl-1,2,4-triazin-5-yl)-2-phenyl-1,2-dicarba-closo-dodecaborane and 1,7-bis[6-phenyl-3-(4-chlorophenyl)-1,2,4-triazin-5-yl]-1,7-dicarba-closo-dodecaborane

Oleg N. Chupakhin,*^a Anton M. Prokhorov,^a Dmitry N. Kozhevnikov,^a Vladimir L. Rusinov,^a Valery N. Kalinin,^b Valentina A. Olshevskaya,^b Ivan V. Glukhov^b and Mikhail Yu. Antipin^b

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* Corresponding authors

^a Department of Chemistry, Urals State Technical University, Ekaterinburg, Russian Federation, , Ekaterinburg, Russian Federation
E-mail: chupakhin@ios.uran.ru

^b A.N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow, Russian Federation, ul. Vavilova, 28, Moscow, Russian Federation

Abstract

The S_N^Hreactions of the lithio derivatives of 1,2- or 1,7-dicarba-closo-dodecaboranes with 1,2,4-triazine 4-oxides represent a versatile synthetic approach to carboranes bearing heteroaromatic substituents.

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DOI: https://doi.org/10.1070/MC2003v013n04ABEH001773
Article type: Communication
Submitted: 22 Apr 2003

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Mendeleev Commun., 2003,13, 165-167

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1,2,4-Triazinylcarboranes: a new approach to the synthesis and the crystal structures of 1-(3,6-ditolyl-1,2,4-triazin-5-yl)-2-phenyl-1,2-dicarba-closo-dodecaborane and 1,7-bis[6-phenyl-3-(4-chlorophenyl)-1,2,4-triazin-5-yl]-1,7-dicarba-closo-dodecaborane

O. N. Chupakhin, A. M. Prokhorov, D. N. Kozhevnikov, V. L. Rusinov, V. N. Kalinin, V. A. Olshevskaya, I. V. Glukhov and M. Yu. Antipin, Mendeleev Commun., 2003, 13, 165 DOI: 10.1070/MC2003v013n04ABEH001773

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Mendeleev Communications

1,2,4-Triazinylcarboranes: a new approach to the synthesis and the crystal structures of 1-(3,6-ditolyl-1,2,4-triazin-5-yl)-2-phenyl-1,2-dicarba-closo-dodecaborane and 1,7-bis[6-phenyl-3-(4-chlorophenyl)-1,2,4-triazin-5-yl]-1,7-dicarba-closo-dodecaborane

Abstract

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1,2,4-Triazinylcarboranes: a new approach to the synthesis and the crystal structures of 1-(3,6-ditolyl-1,2,4-triazin-5-yl)-2-phenyl-1,2-dicarba-closo-dodecaborane and 1,7-bis[6-phenyl-3-(4-chlorophenyl)-1,2,4-triazin-5-yl]-1,7-dicarba-closo-dodecaborane

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