Issue 3, 2003

Crystal structure and magnetic properties of novel chiral nitroxides existing as racemic conglomerates

Abstract

Racemic samples of novel chiral cyclic nitroxides 2-(4-hydroxyphenyl)-2,5,5-trimethylpyrrolidine-1-oxy 1, trans-2-(4-hydroxyphenyl)-2,5-dimethyl-5-phenylpyrrolidine-1-oxy 2 and trans-2,5-bis(4-hydroxyphenyl)-2,5-dimethylpyrrolidine-1-oxy 3 having 4-hydroxyphenyl groups on the stereogenic centres adjacent to the NO radical moiety have been found to exist as racemic conglomerates in the crystalline state, and the origin of the conglomerate formation has been studied by X-ray crystallographic analysis and magnetic susceptibility measurements.

Article information

Article type
Communication
Submitted
28 Apr 2003

Mendeleev Commun., 2003,13, 109-111

Crystal structure and magnetic properties of novel chiral nitroxides existing as racemic conglomerates

N. Ikuma, R. Tamura, S. Shimono, N. Kawame, O. Tamada, N. Sakai, J. Yamauchi and Y. Yamamoto, Mendeleev Commun., 2003, 13, 109 DOI: 10.1070/MC2003v013n03ABEH001787

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