Issue 2, 2003
From the journal:

Mendeleev Communications

Synthesis and properties of benzo[b]thiopheno[2,3-d]-1,3,2λ5-diazaphosphinane-2-thione derivatives

Dmitry B. Nilov*a  and  Vladimir G. Granikb  

* Corresponding authors

a Centre for Medicinal Chemistry. Sergo Ordzhonikidze All-Russian Research Chemical-Pharmaceutical Institute, Moscow, Russian Federation, Zubovskay ul., 7, Moscow, Russian Federation
E-mail: nilov22@hotmail.com

b Russian Research Centre 'Research Institute of Organic Intermediates and Dyes', Moscow, Russian Federation, B.Sadovaya, 1/4, Moscow, Russian Federation

Abstract

The treatment of 2-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylic acid amide with phosphorus pentasulfide in the presence of pyridine yielded 4,5,6,7-tetrahydrobenzo[b]thiopheno[2,3-d]-1,3,2λ5-diazaphosphinane-2-thione; the alkylation of its sodium salts was studied.

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Article information

DOI
https://doi.org/10.1070/MC2003v013n02ABEH001705
Article type
Paper
Submitted
20 Dec 2002

Mendeleev Commun., 2003,13, 78-79

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Synthesis and properties of benzo[b]thiopheno[2,3-d]-1,3,2λ5-diazaphosphinane-2-thione derivatives

D. B. Nilov and V. G. Granik, Mendeleev Commun., 2003, 13, 78 DOI: 10.1070/MC2003v013n02ABEH001705

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