Issue 18, 2003
From the journal:

Chemical Communications

Tris(triphenylplumbyl)plumbate: an anion with three stretched lead–lead bonds

Frank Stabenow,a   Wolfang Saaka  and  Manfred Weidenbruch*a  

* Corresponding authors

a Fachbereich Chemie, Universität Oldenburg, D-26111 Oldenburg, Germany

Abstract

Treatment of lead(II) bromide with phenylmagnesium bromide at low temperature furnishes yellow crystals of the ionic compound [BrMg(THF)5]+ [:Pb(PbPh3)3]− which, upon X-ray crystallographic analysis, reveals three stretched Pb–Pb bonds and Pb–Pb–Pb angles of about 93°.

Graphical abstract: Tris(triphenylplumbyl)plumbate: an anion with three stretched lead–lead bonds

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Article information

DOI
https://doi.org/10.1039/B305217F
Article type
Communication
Submitted
09 May 2003
Accepted
25 Jul 2003
First published
11 Aug 2003

Chem. Commun., 2003, 2342-2343

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Tris(triphenylplumbyl)plumbate: an anion with three stretched lead–lead bonds

F. Stabenow, W. Saak and M. Weidenbruch, Chem. Commun., 2003, 2342 DOI: 10.1039/B305217F

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