Issue 7, 2003
From the journal:

Chemical Communications

Ab initio structure study from in-house powder diffraction of a novel ZnS(EN)0.5 structure with layered wurtzite ZnS fragment

Xiang Ouyang,a   Tsung-Yen Tsai,bd   Dong-Hwang Chen,c   Qi-Jie Huang,b   Wu-Hsun Chengb  and  Abraham Clearfielda  

a Department of Chemistry, Texas A&M University, College Station, TX 77843, USA

b Industrial Technology Research Institute of Taiwan, Hsinchu, ROC

c Department of Chemical Engineering, National Cheng Kung University, Tainan City, Taiwan 70101, ROC

d Centre for Nanotechnology, Chung Yuan Christian University, Chung-Li, Taiwan, ROC

Abstract

The solvothermal reaction of elemental zinc with sulfur in ethylenediamine (en) as solvent yields [ZnS·0.5(NH2CH2CH2NH2)], 1, an unprecedented ethylenediamine pillared ZnS layered compound, containing two dimensional (2-D) boat-type 6-membered rings, which was characterized by ab initio structure solution from powder diffraction data (SDPD).

Graphical abstract: Ab initio structure study from in-house powder diffraction of a novel ZnS(EN)0.5 structure with layered wurtzite ZnS fragment

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Article information

DOI
https://doi.org/10.1039/B212335P
Article type
Communication
Submitted
26 Nov 2002
Accepted
17 Jan 2003
First published
10 Mar 2003

Chem. Commun., 2003, 886-887

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Ab initio structure study from in-house powder diffraction of a novel ZnS(EN)0.5 structure with layered wurtzite ZnS fragment

X. Ouyang, T. Tsai, D. Chen, Q. Huang, W. Cheng and A. Clearfield, Chem. Commun., 2003, 886 DOI: 10.1039/B212335P

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