Issue 5, 2002

Organic synthesis in solid media. Solvent-free Horner–Wadsworth–Emmons reaction in silica gel

Abstract

Silica gel was found to be an excellent medium for the aldehyde-selective Horner-Wadsworth-Emmons reaction, which proceeds at room temperature in a short period of time under solvent-free conditions. The silica gel used for the reaction can be recovered and reused many times without losing its activity.

Graphical abstract: Organic synthesis in solid media. Solvent-free Horner–Wadsworth–Emmons reaction in silica gel

Article information

Article type
Paper
Submitted
29 May 2002
First published
24 Sep 2002

Green Chem., 2002,4, 498-500

Organic synthesis in solid media. Solvent-free Horner–Wadsworth–Emmons reaction in silica gel

Y. Z. Jin, N. Yasuda and J. Inanaga, Green Chem., 2002, 4, 498 DOI: 10.1039/B205239C

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