Issue 3, 2001
From the journal:

Green Chemistry

Efficient solvent-free O-silylation of alcohols with R3SiCl

Bunpei Hatano,a   Shinji Toyotaa  and  Fumio Toda*a  

* Corresponding authors

a Department of Chemistry, Faculty of Science, Okayama University of Science, Ridai-cho 1-1, 700-0005, Okayama, Japan.
E-mail: toda@chem.ous.ac.jp

Abstract

Solvent-free O-silylation of liquid or crystalline alcohols with liquid or crystalline silyl chlorides proceeds efficiently to give silyl ethers in good yield. O-Silylation of sterically hindered alcohols which cannot be performed in solution is also accomplished efficiently under solvent-free conditions.

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Article information

DOI
https://doi.org/10.1039/B102447G
Article type
Paper
Submitted
15 Mar 2001
First published
30 May 2001

Green Chem., 2001,3, 140-142

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Efficient solvent-free O-silylation of alcohols with R3SiCl

B. Hatano, S. Toyota and F. Toda, Green Chem., 2001, 3, 140 DOI: 10.1039/B102447G

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