Issue 19, 2001
From the journal:

Journal of the Chemical Society, Dalton Transactions

Synthesis and structure of an aluminium 3-aminopropylphosphonate sulfate hydrate

Nadja Zakowsky,a   Paul S. Wheatley,a   Ivor Bull,a   Martin P. Attfieldb  and  Russell E. Morris*a  

* Corresponding authors

a School of Chemistry, University of St. Andrews, Purdie Building, St. Andrews, UK
E-mail: rem1@st-and.ac.uk

b School of Crystallography, Birkbeck College, University of London, Malet Street, London, UK

Abstract

A new aluminium 3-aminopropylphosphonate sulfate hydrate has been prepared using hydrothermal methods, and its structure solved using microcrystal X-ray diffraction at a synchrotron source. The structure consists of one-dimensional chains of aluminium 3-aminopropylphosphonate with sulfate anions occluded between the chains. It is unusual in compounds of this type to have anionic groups between positively charged aluminium phosphonate units. Further characterisation of the compound has been carried out using magic angle spinning NMR.

Graphical abstract: Synthesis and structure of an aluminium 3-aminopropylphosphonate sulfate hydrate

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Article information

DOI
https://doi.org/10.1039/B103911N
Article type
Paper
Submitted
01 May 2001
Accepted
09 Jul 2001
First published
11 Sep 2001

J. Chem. Soc., Dalton Trans., 2001, 2899-2902

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Synthesis and structure of an aluminium 3-aminopropylphosphonate sulfate hydrate

N. Zakowsky, P. S. Wheatley, I. Bull, M. P. Attfield and R. E. Morris, J. Chem. Soc., Dalton Trans., 2001, 2899 DOI: 10.1039/B103911N

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