Resolving multiple 27Al sites in AlVO4 by 27Al MAS NMR spectroscopy at 21.15 Tesla

Ulla Gro Nielsen; Jørgen Skibsted; Hans J. Jakobsen

doi:10.1039/B109042A

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Resolving multiple ²⁷Al sites in AlVO₄ by ²⁷Al MAS NMRspectroscopy at 21.15 Tesla

Ulla Gro Nielsen,^a Jørgen Skibsted^a and Hans J. Jakobsen*^a

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* Corresponding authors

^a Instrument Centre for Solid-State NMR Spectroscopy, Department of Chemistry, University of Aarhus, Langelandsgade 140, Aarhus, Denmark.
E-mail: ulla@chem.au.dk; jskib@chem.au.dk; hja@chem.au.dk

Abstract

A high-resolution 21.15 Tesla magnet (900 MHz for ¹H NMR) along with a home-built CP/MAS NMR probe is employed to succesfully resolve three different ²⁷Al resonances in AlVO₄, allowing a precise determination of their quadrupole coupling parameters and isotropic chemical shifts.

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Article information

DOI: https://doi.org/10.1039/B109042A
Article type: Communication
Submitted: 05 Oct 2001
Accepted: 14 Nov 2001
First published: 04 Dec 2001

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Chem. Commun., 2001, 2690-2691

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Resolving multiple ²⁷Al sites in AlVO₄ by ²⁷Al MAS NMR spectroscopy at 21.15 Tesla

U. G. Nielsen, J. Skibsted and H. J. Jakobsen, Chem. Commun., 2001, 2690 DOI: 10.1039/B109042A

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