Short syntheses of enantiopure calystegineB2, B3, and B4

Philip R. Skaanderup; Robert Madsen

doi:10.1039/B102353P

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Short syntheses of enantiopure calystegine B₂, B₃, and B₄

Philip R. Skaanderup^a and Robert Madsen*^a

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* Corresponding authors

^a Department of Chemistry, Technical University of Denmark, Building 201, Lyngby, Denmark.
E-mail: rm@kemi.dtu.dk

Abstract

Calystegine B₂, B₃, and B₄ have been prepared in 5 steps from the benzyl protected methyl 6-iodoglycopyranosides of glucose, galactose and mannose, respectively, by using a zinc-mediated domino reaction followed by ring-closing olefin metathesis as the key steps.

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Article information

DOI: https://doi.org/10.1039/B102353P
Article type: Communication
Submitted: 12 Mar 2001
Accepted: 26 Apr 2001
First published: 31 May 2001

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Chem. Commun., 2001, 1106-1107

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Short syntheses of enantiopure calystegine B₂, B₃, and B₄

P. R. Skaanderup and R. Madsen, Chem. Commun., 2001, 1106 DOI: 10.1039/B102353P

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