15N NMR and crystal structure studies of 5-(2-pyridylmethylene)pseudothiohydantoin; dipolar dephasing experiments for establishing the preferred tautomer in the solid and solution states

Mubarik M. Chowdhry; D. Michael P. Mingos; Andrew J. P. White; David J. Williams

doi:10.1039/B004368K

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¹⁵N NMR and crystal structure studies of 5-(2-pyridylmethylene)pseudothiohydantoin;† dipolar dephasing experiments for establishing the preferred tautomer in the solid and solution states

Mubarik M. Chowdhry,‡^a D. Michael P. Mingos,§*^a Andrew J. P. White^a and David J. Williams^a

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^a Department of Chemistry, Imperial College of Science, Technology and Medicine, South Kensington, London, UK

Abstract

The preferred tautomeric form of 5-(2-pyridylmethylene)pseudothiohydantoin 1 in the solid and solution states has been determined by natural abundance high-resolution ¹⁵N NMR studies and by a single crystal X-ray structural analysis.

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Supplementary files

Crystal structure data TXT (11K)

Article information

DOI: https://doi.org/10.1039/B004368K
Article type: Paper
Submitted: 01 Jun 2000
Accepted: 14 Aug 2000
First published: 09 Oct 2000

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J. Chem. Soc., Perkin Trans. 2, 2000, 2265-2268

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¹⁵N NMR and crystal structure studies of 5-(2-pyridylmethylene)pseudothiohydantoin; dipolar dephasing experiments for establishing the preferred tautomer in the solid and solution states

M. M. Chowdhry, D. M. P. Mingos, A. J. P. White and D. J. Williams, J. Chem. Soc., Perkin Trans. 2, 2000, 2265 DOI: 10.1039/B004368K

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Journal of the Chemical Society, Perkin Transactions 2