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Issue 14, 2000
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Stereoselective synthesis of α-L-Fucp-(1,2)- and -(1,3)-β-D-Galp(1)-4-methylumbelliferone using glycosyl donor substituted by propane-1,3-diyl phosphate as leaving group

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Abstract

The synthesis of the disaccharides α-L-Fucp-(1,2)- and α-L-Fucp-(1,3)-β-D-Galp(1)-4-methylumbelliferone as fucosidase substrates was accomplished by activation of the anomeric centre of 2,3,4-tri-O-acetyl- and 2,3,4,6-tetra-O-acetyl-α,β-L-fuco- and -D-galactopyranosyl propane-1,3-diyl phosphates with TMSOTf and with minimal protection of 4-methylumbelliferyl β-D-galactopyranoside.

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Publication details

The article was received on 06 Apr 2000, accepted on 02 Jun 2000 and first published on 27 Jun 2000


Article type: Paper
DOI: 10.1039/B002754P
Citation: J. Chem. Soc., Perkin Trans. 1, 2000,0, 2187-2193

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    Stereoselective synthesis of α-L-Fucp-(1,2)- and -(1,3)-β-D-Galp(1)-4-methylumbelliferone using glycosyl donor substituted by propane-1,3-diyl phosphate as leaving group

    H. Vankayalapati and G. Singh, J. Chem. Soc., Perkin Trans. 1, 2000, 0, 2187
    DOI: 10.1039/B002754P

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