The synthesis is reported of the first rotaxane involving a bound ferrocenyl moiety and β-cyclodextrin; cyclodextrin groups are used as stoppers; intermediate 1:1 adduct formation in d8-THF was monitored by HR-DOSY methods (Kd=25 mM, 293 K) and the product rotaxane, isolated in 11% yield, has been characterised by NMR, CD and MALDI-TOF MS.
P. J. Skinner, S. Blair, R. Kataky and D. Parker, New J. Chem., 2000, 24, 265 DOI: 10.1039/B000438N
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