Arylmethaniminyl and alkyl radicals were generated from di- and tri-methoxyphenyl aldoxime esters, by photolysis in the presence of 4-methoxyacetophenone, and were detected by EPR spectroscopy: good yields of cyclised products were isolated from suitably unsaturated alkyl substituents.
Enhanced radical delivery from aldoxime esters for EPR and ring closure applications
A. J. McCarroll and J. C. Walton, Chem. Commun., 2000, 351 DOI: 10.1039/A910346P
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