Issue 5, 2000
From the journal:

Chemical Communications

Covalent capture of dynamic hydrogen-bonded assemblies

F. Cardullo,a   M. Crego Calama,a   B. H. M. Snellink-Ruël,a   J.-L. Weidmann,a   A. Bielejewska,a   R. Fokkens,b   N. M. M. Nibbering,b   P. Timmerman*a  and  D. N. Reinhoudt*a  

* Corresponding authors

a Laboratory of Supramolecular Chemistry and Technology, MESA+ Research Institute, University of Twente, PO Box 217, Enschede, The Netherlands.
E-mail: d.n.reinhoudt@ct.utwente.nl.

b Institute of Mass Spectrometry, University of Amsterdam, Nieuwe Achtergracht 129, Amsterdam, The Netherlands

Abstract

Covalent linkage of the three calix[4]arene units in hydrogen-bonded assemblies 13•(DEB)6via a threefold ring closing metathesis (RCM) reaction quantitatively converts the dynamic assemblies into covalent systems (123-membered macrocycles) that can be easily characterized using MALDI-TOF MS and HPLC.

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Article information

DOI
https://doi.org/10.1039/A909459H
Article type
Communication
Submitted
26 Nov 1999
Accepted
18 Jan 2000
First published
22 Feb 2000

Chem. Commun., 2000, 367-368

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Covalent capture of dynamic hydrogen-bonded assemblies

F. Cardullo, M. C. Calama, B. H. M. Snellink-Ruël, J.-L. Weidmann, A. Bielejewska, R. Fokkens, N. M. M. Nibbering, P. Timmerman and D. N. Reinhoudt, Chem. Commun., 2000, 367 DOI: 10.1039/A909459H

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