SCHEDULED MAINTENANCE
The iodine–lithium exchange reaction on the 1,1-diiodoalkanes 17 at –110 °C is initiated by the irreversible formation of yellow iodine ate-complexes, which are slowly transformed into the α-iodoalkyllithium compounds 21.
M. Müller, H. Stiasny, M. Brönstrup, A. Burton and R. W. Hoffmann, J. Chem. Soc., Perkin Trans. 2, 1999, 731 DOI: 10.1039/A900121B
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