The TiCl4- or SnCl4-promoted cyclization of homoallylic alcohols with malonaldehyde bis(dimethylacetal) affords bis(2-tetra-hydropyranyl)methane derivatives, which are potential precursors of C-(1→1)-disaccharides and other cyclic polyethers.
V. V. Samoshin, D. E. Gremyachinskiy and P. H. Gross, Mendeleev Commun., 1999, 9, 53 DOI: 10.1070/MC1999v009n02ABEH001087
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