The preparation of Ph3P(SCN)2 is modified by using a combination of Ph3P, NH4SCN and Br2 at room temperature for the efficient conversion of primary, secondary and tertiary alcohols to their corresponding thiocyanates in excellent yields.
N. Iranpoor, H. Firouzabadi and H. R. Shaterian, J. Chem. Res. (S), 1999, 676 DOI: 10.1039/A906113D
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