Synthesis of diacetals in excellent yields from aldehydes and ketones with 2,2-bis(hydroxymethyl)propane-1,3-diol is carried out in refluxing benzene or toluene with anhydrous ferrous sulfate as catalyst.
T. Jin, Y. Ma, T. Li and J. Wang, J. Chem. Res. (S), 1999, 268 DOI: 10.1039/A900025I
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