The first metal coordination polymer containing3,4′-bipyridine (3,4′-bpy) was prepared by the hydrothermal treatment of Cu(NO3)2·2.5H2O, Me3SnBr and3,4′-bpy and its crystal structure shows a infinite double chain composed of two 3,4′-bpy and Br as well as copper(I) ions with an approximately rectangular molecular box of 4.0 × 10.68 Å.
H. Fun, S. Shanmuga Sundara Raj, R. Xiong, J. Zuo, Z. Yu, X. Zhu and X. You, J. Chem. Soc., Dalton Trans., 1999, 1711 DOI: 10.1039/A902054C
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