The complex [Cu{2,6-di(pyrazol-1-yl)pyridine}2](BF4)2 undergoes a solid-state phase transition at 41 K, involving the cooperative ordering of its planar dynamic pseudo-Jahn–Teller system; this unique phase transition is characterised by single-crystal X-ray diffraction techniques, employing an open-flow helium cryostat.
M. A. Leech, J. A. K. Howard, S. Dahaoui, N. K. Solanki and M. A. Halcrow, Chem. Commun., 1999, 2245 DOI: 10.1039/A906876G
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