2,2-Difluoro enol silyl ethers were readily prepared by Mg0 promoted selective defluorination of trifluoromethyl ketones in the presence of TMSCl, which involves C–F bond cleavage.
H. Amii, T. Kobayashi, Y. Hatamoto and K. Uneyama, Chem. Commun., 1999, 1323 DOI: 10.1039/A903681D
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