The first example of a stabilized diaminophonium diazaylide, sodium diphenylbis(cyanamido)phosphonium diylide, has been synthesized by a new variation of the Staudinger reaction; the corresponding copper complex can be described as a discrete dimeric unit with [Ph2P(NCN)2]– in both uni- and bi-dentate modes (X-ray structure).
M. Taillefer, N. Inguimbert, H. Cristau, L. Jäger and K. Merzweiler, Chem. Commun., 1999, 565 DOI: 10.1039/A808641I
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