A potentially toxophoric subunit of methyllycaconitine has been synthesised from penta-1,4-dien-3-ol as the mixture of diastereomers 2a and 2b, in 14 steps and 5% overall yield.
L. C. Baillie, J. R. Bearder, W. Li, J. A. Sherringham and D. A. Whiting, J. Chem. Soc., Perkin Trans. 1, 1998, 4047 DOI: 10.1039/A807760F
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