The synthesis of enantiopure A-factor [‘autoregulatory factor’; (3R)-(–)-2-(6-methylheptanoyl)-3-hydroxymethylbutano-4-lactone] by the completely diastereoselective benzyloxymethylation of (4R)-3-(3-phenylpropanoyl)-4-isopropyloxazolidin-2-one is reported.
J. M. Crawforth, J. Fawcett and B. J. Rawlings, J. Chem. Soc., Perkin Trans. 1, 1998, 1721 DOI: 10.1039/A708638E
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