The X-ray structure of a single crystal of the neutral donor 1b and its electrocrystallized cation radical salt, 1b·ClO4, have been analysed. Both the neutral and the oxidized states adopt a syn conformation stabilized by strong intramolecular interactions that allow the preservation of a planar conformation during the oxidation of 1b.
E. Hadj Elandaloussi, P. Frère, P. F. ,. A. R. J. R., A. Riou and J. Roncali, New J. Chem., 1998, 22, 1051 DOI: 10.1039/A803213K
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