Single phase Na5H(CN2)3 was obtained by thermal decomposition of Na(HNCN) and structurally characterized by Rietveld refinement of X-ray powder diffraction data; Na5H(CN2)3 was found to be isostructural to K5H(CN2)3, and identical to a phase that was previously reported as ‘Na4H2(CN)3‘.
M. Becker and M. Jansen, J. Chem. Res. (S), 1998, 86 DOI: 10.1039/A706196J
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