Chemical dehydrochlorination of 1,1,1-trichloroethane with anhydrous KOH in the presence of a poly(ethylene glycol) oligomer as phase transfer catalyst leads to the formation of carbyne particles with diameters in the range of 30–50 nm.
G. Shi, Chem. Commun., 1998, 2271 DOI: 10.1039/A805244A
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