The facile preparation of macrocyclic ethers is achieved using S NAr reactions of (dichlorobenzene)CpFe + complexes with various dinucleophiles, followed by photolytic demetallation; X-ray crystallography gives unequivocal structural proof for one of these macrocycles.
A. S. Abd-El-Aziz, C. R. de Denus, M. J. Zaworotko and C. V. Krishnamohan Sharma, Chem. Commun., 1998, 265 DOI: 10.1039/A704333C
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