Synthesis of the aromatic unit of calicheamicinγ1I

Yong-Zhou Hu; Derrick L. J. Clive

doi:10.1039/A605837J

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Synthesis of the aromatic unit of calicheamicin γ₁^I

Yong-Zhou Hu and Derrick L. J. Clive

Abstract

Vanillin and piperonal are each converted into methyl 2,3-dimethoxy-6-methyl-4-(prop-2-enyl)benzoate 12, and this is then elaborated into methyl 4-hydroxy-3-iodo-5,6-dimethoxy-2-methylbenzoate 24, which represents the aromatic unit of calicheamicin γ₁^I.

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DOI: https://doi.org/10.1039/A605837J
Article type: Paper

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J. Chem. Soc., Perkin Trans. 1, 1997, 1421-1424

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Synthesis of the aromatic unit of calicheamicin γ₁^I

Y. Hu and D. L. J. Clive, J. Chem. Soc., Perkin Trans. 1, 1997, 1421 DOI: 10.1039/A605837J

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Journal of the Chemical Society, Perkin Transactions 1

Synthesis of the aromatic unit of calicheamicin γ₁^I

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Synthesis of the aromatic unit of calicheamicin γ₁^I

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Journal of the Chemical Society, Perkin Transactions 1