The structure determination of [Zn2L][CF3SO3]2 1 reveals the first example of non-bridging thiolates within a thiolate-containing Schiff-base macrocyclic complex: the flexibility of such macrocycles is also clearly demonstrated as this is the first example of the provision of distorted tetrahedral metal ion binding sites.
S. Brooker and T. C. Davidson, Chem. Commun., 1997, 2007 DOI: 10.1039/A705415G
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