SCHEDULED MAINTENANCE
X-Ray crystallographic structure of Ga8(pz)12O4Cl4·2thf: a novel gallium pyrazololate complex with a Ga4O4 core
Abstract
The reaction of Na[MeGa(pz)
3
] with GaCl
3
leads to
the formation of the novel cubane
Ga
8
(pz)
12
O
4
Cl
4
·2thf 1,
and not the expected product
[{MeGa(pz)
3
}
2
Ga][GaCl
4
]; the
ease with which 1 forms is illustrated by its formation in a subsequent
reaction of Na[MeGa(pz)
3
] with GaCl
3
.
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