SCHEDULED MAINTENANCE
We report the first synthesis of β-2′-deoxy[9-15N] adenosine: the last of the singly labelled 5N β-2′-deoxyadenosines to be synthesized. Using commercially available 5-amino-4,6-dichloropyrimidine and 2–10 equivalents of 15NH3, β-2′-deoxy[9-15N]adenosine has been constructed in four steps in good overall yield.
C. C. Orji, J. Kelly, D. A. Ashburn and L. A. Silks, J. Chem. Soc., Perkin Trans. 1, 1996, 595 DOI: 10.1039/P19960000595
To request permission to reproduce material from this article, please go to the Copyright Clearance Center request page.
If you are an author contributing to an RSC publication, you do not need to request permission provided correct acknowledgement is given.
If you are the author of this article, you do not need to request permission to reproduce figures and diagrams provided correct acknowledgement is given. If you want to reproduce the whole article in a third-party publication (excluding your thesis/dissertation for which permission is not required) please go to the Copyright Clearance Center request page.
Read more about how to correctly acknowledge RSC content.
Please wait while we load your content...