Reductive deoxygenation of acylferrocenes to the corresponding alkylferrocenes proceeded in excellent yields on utilizing a combination of sodium cyanotrihydroborate and boron trifluoride–diethyl ether. This method allows the synthesis of alkylferrocenes with functionalized tethers and is adaptable to large-scale preparations.
S. Bhattacharyya, J. Chem. Soc., Dalton Trans., 1996, 4617 DOI: 10.1039/DT9960004617
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